View Item 
  •   Unmul Repository Home
  • Akuntabel
  • J - Pharmacy
  • View Item
  •   Unmul Repository Home
  • Akuntabel
  • J - Pharmacy
  • View Item
JavaScript is disabled for your browser. Some features of this site may not work without it.

SYNTHESIS AND CHARACTERIZATION OF METHYL AMINO POLYSTYRENE AS RESIN MATERIAL OF CHROMATOGRAPHY

Thumbnail
View/Open
SYNTHESIS AND CHARACTERIZATION OF METHYL AMINO POLYSTYRENE AS RESIN MATERIAL OF CHROMATOGRAPHY.pdf (2.238Mb)
Date
2018
Author
Herman, Herman
Anggraeni, Anni
Mutalib, Abdul
Bahti, Husein H
Metadata
Show full item record
Abstract
Ion-exchange chromatography has been widely used in various separation process and purification. Commercial ion-exchange resin mostly uses polystyrene as base. This study reviewed the synthesis of cation-exchange resin with polystyrene as starting material. Polystyrene must be activated in order to make one of aromatic carbon chains being able to be binding with acetamide n-hidroxymethyl electrophilic. Polystyrene activation was conducted through two stages, i.e. (1) the formation of amidomethyl polystyrene (AMDP), and followed with (2) hydrolysis of acyl group. The activation of polystyrene generated white methylamino polystyrene (MAP) resin, of which its characterization used spectrophotometry UV, Fourier Transform-Infrared (FTIR), and density of MAP resin confirmed by pycnometer. The results showed that the characterization of FTIR and spectrophotometer UV for AMP exhibited the forming of primary amino group and disappearance of spectrum band of C=O group at 3374.52 cm-1 with λmax 230 nm, the average of density of AMP resin sample was 1.7158 g/mL.
URI
http://repository.unmul.ac.id/handle/123456789/6939
Collections
  • J - Pharmacy [579]

Repository Universitas Mulawarman copyright ©   LP3M Universitas Mulawarman
Jalan Kuaro Kotak Pos 1068
Telp. (0541) 741118
Fax. (0541) 747479 - 732870
Samarinda 75119, Kalimantan Timur, Indonesia
Contact Us | Send Feedback
 

 

Browse

All of Unmul RepositoryCommunities & CollectionsBy Issue DateAuthorsTitlesSubjectsThis CollectionBy Issue DateAuthorsTitlesSubjects

My Account

Login

Repository Universitas Mulawarman copyright ©   LP3M Universitas Mulawarman
Jalan Kuaro Kotak Pos 1068
Telp. (0541) 741118
Fax. (0541) 747479 - 732870
Samarinda 75119, Kalimantan Timur, Indonesia
Contact Us | Send Feedback